The title compound, C(15)H(13)N(3)O(2)S, was synthesized by the reaction of 2-amino-5,6,7,8-tetra-hydro-4H-cyclo-hepta-[b]thio-phene-3-carbonitrile and o-fluoro-nitro-benzene. The dihedral angle between the thio-phene and nitro-phenyl rings is 75.15â (2)°. In the crystal, inter-molecular N-Hâ¯N and C-Hâ¯O inter-actions lead to the formation of a supra-molecular chain extending along the c-axis direction.
2-(2-Nitro-anilino)-4,5,6,7-tetra-hydro-benzo[b]thio-phene-3-carbonitrile.
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作者:Mendonça Junior Francisco J B, de Lima Maria do Carmo A, Galdino Suely L, Pitta Ivan R, de Simone Carlos A
| 期刊: | Acta Crystallographica Section E-Structure Reports Online | 影响因子: | 0.600 |
| 时间: | 2010 | 起止号: | 2010 Sep 11; 66(Pt 10):o2543 |
| doi: | 10.1107/S1600536810035439 | ||
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