In the title solvate, C22H18O6·2C3H7NO, the complete dicarboxylic acid molecule is generated by a crystallographic twofold axis, which bisects the central benzene ring and one N,N-di-methyl-formamide solvent mol-ecule. The dihedral angle between the central and pendant benzene rings is 54.53â (5)° while that between the pendant rings is 45.44â (5)°. In the crystal, the acid molecules are linked to the solvent molecules via O-Hâ¯O and weak C-Hâ¯O hydrogen bonds. Further weak C-Hâ¯O inter-actions link adjacent acid mol-ecules into a three-dimensional network.
4,4'-{[1,2-Phenyl-enebis(methyl-ene)]bis-(-oxy)}di-benzoic acid di-methyl-formamide disolvate.
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作者:Qiu Zhen-Zhe, Jing Bi, Li Qiu-Xia, Zhu Ai-Xin
| 期刊: | Acta Crystallographica Section E-Structure Reports Online | 影响因子: | 0.600 |
| 时间: | 2014 | 起止号: | 2014 Apr 12; 70(Pt 5):o534-5 |
| doi: | 10.1107/S1600536814006795 | ||
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