In the title compound, C(28)H(26)Cl(2)N(4)O(4)S, the dihedral angles between the two chloro-phenyl rings and the two oxadiazol rings are 10.51â (4)° and 13.55â (3)°, respectively. The thio-phene ring is oriented at dihedral angles of 5.59â (4)°, 8.33â (4)° and 4.41â (4)°, 11.05â (3)°, respectively, with respect to the two oxadiazol and the two chloro-phenyl rings. The intra-molecular C-Hâ¯O hydrogen bond results in the formation of a five-membered ring. In the crystal structure, Ï-Ï contacts between the oxadiazol rings, the chloro-phenyl rings and the chloro-phenyl and oxadiazol rings [centroid-centroid distances = 3.428â (3)â à , 3.750â (3)â à and 3.768â (3)â à , respectively] are present.
2-(4-Chloro-phen-yl)-5-{3,4-dibut-oxy-5-[5-(4-chloro-phen-yl)-1,3,4-oxadiazol-2-yl]thio-phen-2-yl}-1,3,4-oxadiazole.
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作者:Li Hai-Lin, Wang Hong-Wei, Lu Ran-Zhe, Wang Hai-Bo
| 期刊: | Acta Crystallographica Section E-Structure Reports Online | 影响因子: | 0.600 |
| 时间: | 2008 | 起止号: | 2008 Nov 8; 64(Pt 12):o2298 |
| doi: | 10.1107/S1600536808035848 | ||
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