In the title compound, C40H30Cl2N2O4, the two benzene rings of the biphenyl unit are twisted with respect to each other, making a dihedral angle of 73.07â (4)°. The benzene rings of the benzamide groups form dihedral angles of 77.09â (5) and 55.48â (6)° with the central biphenyl moiety. In the crystal, mol-ecules are linked through N-Hâ¯O hydrogen bonds to form a fused R 2 (2)(38) ring motif which forms a supermolecular ribbon network extending along the [100] plane. In the two 4-chloro-phenyl rings, the five C atoms and their attached H atoms are disordered over two sets of sites, with site-occupancy factors of 0.657â (15):0.343â (15) and 0.509â (13):0.491â (13).
3,3'-{[(Biphenyl-2,2'-di-yl)bis-(methyl-ene)]bis-(-oxy)}bis-[N-(4-chloro-phen-yl)benzamide].
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作者:Rajadurai Raj, Padmanabhan Ramar, Meenakshi Sundaram Soma Sundaram, Ananthan Sarkkarai
| 期刊: | Acta Crystallographica Section E-Structure Reports Online | 影响因子: | 0.600 |
| 时间: | 2013 | 起止号: | 2013 May 18; 69(Pt 6):o914-5 |
| doi: | 10.1107/S160053681301009X | ||
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