2-Chloro-N-methyl-N-[2-(methyl-amino)-phen-yl]acetamide.

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作者:Bai Yu-Bin, Chen Xia-Hui, Ma Ya-Tuan, Zhang An-Ling, Gao Jin-Ming
The title compound, C(10)H(13)ClN(2)O, was obtained as a by-product in the reaction of 2-chloro-methyl-1H-benzimidazole, dimethyl sulfate and toluene to synthesise 2-chloro-methyl-1-methyl-benzimidazole. The dihedral angle between the benzene ring and the acetamide group is 89.72 †(6)° while that between the aromatic ring and the chloracetyl group is 84.40†(4)°. In the crystal, adjacent mol-ecules are linked by pairs of N-H⋯O hydrogen bonds into inversion dimers.

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