The title compound, C(10)H(13)ClN(2)O, was obtained as a by-product in the reaction of 2-chloro-methyl-1H-benzimidazole, dimethyl sulfate and toluene to synthesise 2-chloro-methyl-1-methyl-benzimidazole. The dihedral angle between the benzene ring and the acetamide group is 89.72 â (6)° while that between the aromatic ring and the chloracetyl group is 84.40â (4)°. In the crystal, adjacent mol-ecules are linked by pairs of N-Hâ¯O hydrogen bonds into inversion dimers.
2-Chloro-N-methyl-N-[2-(methyl-amino)-phen-yl]acetamide.
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作者:Bai Yu-Bin, Chen Xia-Hui, Ma Ya-Tuan, Zhang An-Ling, Gao Jin-Ming
| 期刊: | Acta Crystallographica Section E-Structure Reports Online | 影响因子: | 0.600 |
| 时间: | 2013 | 起止号: | 2013 Feb 1; 69(Pt 2):o229 |
| doi: | 10.1107/S1600536813000494 | ||
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