The title compound, C(21)H(21)N(3)O, was obtained by cyclo-condensation of 3-amino-5-methyl-[1,1'-biphen-yl]-2,4-di-car-bo-nitrile with cyclo-hexa-none. The six-membered 1,3-diaza ring assumes an envelope conformation [with the flap atom displaced by 0.511â (7)â à from the plane through the other ring atoms] and the cyclo-hexane ring displays a chair conformation. The dihedral angle between the aromatic rings is 42.61â (7)°.In the crystal, the mol-ecules form hydrogen-bonded bands along [011].
5'-Methyl-4'-oxo-7'-phenyl-3',4'-dihydro-1'H-spiro-[cyclo-hexane-1,2'-quinazoline]-8'-carbonitrile.
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作者:Tang Jianhong, Shi Daxin, Yan Liupan, Liu Xuan, Li Jiarong
| 期刊: | Acta Crystallographica Section E-Structure Reports Online | 影响因子: | 0.600 |
| 时间: | 2011 | 起止号: | 2011 Jul 1; 67(Pt 7):o1672 |
| doi: | 10.1107/S160053681102188X | ||
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