The majority of the title mol-ecule, C(28)H(34)ClN(3)O(9)S, is disordered over two closely spaced sets of sites; the site occupancy of the major component = 0.542â (3). The conformation of each component is approximately U-shaped with the chloro-benzene ring forming the base and the indolinyl and sulfamoyl groups the sides; an intra-molecular C-Hâ¯Cl hydrogen bond possibly contributes to the stabilization of the conformation. In the crystal, a corrugated layer structure parallel to the ab plane is formed by C-Hâ¯O and C-Hâ¯Cl hydrogen bonds together with C-Hâ¯Ï(ring) inter-actions.
Diethyl 2,2'-[({2-chloro-5-[(2-eth-oxy-2-oxoeth-yl)(2-methyl-indolin-1-yl)carbamo-yl]phen-yl}sulfon-yl)aza-nedi-yl]di-acetate.
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作者:Ramli Youssef, Al Garadi Wedad, El Hafi Mohamed, Lhoussaine Elghayati, Essassi El Mokhtar, Alsubari Abdulsalam, Mague Joel T
| 期刊: | IUCrdata | 影响因子: | 0.000 |
| 时间: | 2023 | 起止号: | 2023 Aug 24; 8(Pt 8):x230699 |
| doi: | 10.1107/S2414314623006995 | ||
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