Simple Synthesis of CeO(2) Nanoparticle Composites In Situ Grown on Carbon Nanotubes for Phenol Detection

一种用于苯酚检测的碳纳米管原位生长CeO₂纳米颗粒复合材料的简易合成方法

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Abstract

via simple hydrothermal method, CeO(2) was in-situ grown onto the CNTs to form CeO(2)/CNTs nanocomposites were synthesized with cerium nitrate as Ce resource. The morphology and structure were characterized by transmission electron microscopy and X-ray diffraction. The characterizations reveal that CeO(2) nanoparticles are uniformly dispersed onto the surface of the pre-acidified CNTs. The electrochemical property of the synthesized nanocomposite was investigated in 0.1 M KCl electrolyte containing 2 mM [Fe(CN)(6)](3-/4-). The nanocomposites were employed to fabricate electrochemical sensor for phenol detection. The linear range for phenol detection measured by the differential pulse voltammetry method is 1-500 μM. The sensor also exhibits good selectivity, reproducibility and stability. When applied for the river and tap water analysis, it shows good recovery rate.

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