Shape engineering of polystyrene particles from spherical to raspberry-like to hollow flower-like via one-step non-surfactant self-templating polymerization of styrene in ethanol-water mixtures

通过在乙醇-水混合物中一步无表面活性剂自模板聚合苯乙烯,实现聚苯乙烯颗粒从球形到覆盆子状再到空心花状的形状工程

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Abstract

We report a facile method for preparation of polystyrene (PS) particles with spherical, raspberry-like, and hollow flower-like structures by single-step non-surfactant self-templating polymerization of styrene in ethanol-water mixtures. PS particles with diverse morphologies could be easily obtained by simply adjusting the volume ratios of the styrene/water/ethanol mixture and initiator-ethanol-water mixture. By decreasing this ratio, the particles with spherical, raspberry-like, and hollow flower-like structures were obtained in sequence. The wettability of the coatings changing from hydrophilicity to hydrophobicity was easily tuned by the PS particles with different roughnesses. A competitive mechanism of interfacial polymerization and exudation was proposed to interpret the formation of PS particles with diverse morphologies.

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