Preparation and Characterization of Carbide Particle-Toughened Si-B System of High Thermostability Polycrystalline Diamond by HPHT Sintering

采用高温高压烧结法制备和表征碳化物颗粒增韧的高热稳定性Si-B体系多晶金刚石

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Abstract

In this research, we report the synthesis of Si-TmC-B/PCD composites using Si, B, and transition metal carbide particles (TmC) as binders at high pressure and high temperature (HPHT method, 5.5 GPa and 1450 °C). The microstructure, elemental distribution, phase composition, thermal stability, and mechanical properties of PCD composites were systematically investigated. The Si-B/PCD sample is thermally stable in air at 919 °C. The initial oxidation temperature of the PCD sample with ZrC particles is as high as 976 °C, and it also has a maximum flexural strength of 762.2 MPa, and the highest fracture toughness of 8.0 MPa·m(1/2).

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