In the title compound, C(21)H(17)N(5)O(3)S(3)·C(3)H(7)NO, the toluene-sulfonamide ring and the combined ring system involving the pyridone and benzo-thia-zole rings subtend an inter-planar angle of 39.86â (4)°. The pyridone and benzo-thiazyl rings are linked by the intra-molecular hydrogen bond N-H(amine)â¯N(thia-zole). The DMF O atom accepts two classical hydrogen bonds. The mol-ecules are linked by hydrogen bonds and an Sâ¯O contact to form layers parallel to the bc plane.
Crystal structure of N-[6-amino-5-(benzo[d]thia-zol-2-yl)-3-cyano-4-methyl-sulfanyl-2-oxo-1,2-di-hydro-pyridin-1-yl]-4-methyl-benzene-sulfonamide di-methyl-formamide monosolvate.
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作者:Azzam Rasha A, Elgemeie Galal H, Elsayed Rasha E, Jones Peter G
| 期刊: | Acta Crystallographica Section E: Crystallographic Communications | 影响因子: | 0.500 |
| 时间: | 2017 | 起止号: | 2017 Nov 3; 73(Pt 12):1820-1822 |
| doi: | 10.1107/S2056989017015778 | ||
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