The crystal structure of the title compound, C(14)H(12)N(2)O(4), contains four crystallographically independent mol-ecules in the asymmetric unit. All the mol-ecules have similar conformations; the dihedral angles between the aromatic rings are 33.1â (1), 33.76â (9), 31.41â (9) and 32.56â (10)°. Intra-molecular O-Hâ¯N hydrogen bonds form S(6) ring motifs in each molecule. In the crystal, there are two pairs of pseudo-inversion-related mol-ecules. Along the c axis, mol-ecules are stacked with Ï-Ï inter-actions between the 2-hy-droxy-phenyl and 4-meth-oxy-2-nitro-phenyl rings [centroid-centroid distances = 3.5441â (12)-3.7698â (12)â à ].
2-[(4-Meth-oxy-2-nitro-phen-yl)imino-meth-yl]phenol.
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作者:Khalaji Aliakbar Dehno, Nikookar Mahsa, Fejfarová Karla, DuÅ¡ek Michal
| 期刊: | Acta Crystallographica Section E-Structure Reports Online | 影响因子: | 0.600 |
| 时间: | 2012 | 起止号: | 2012 Aug 1; 68(Pt 8):o2445-6 |
| doi: | 10.1107/S1600536812031212 | ||
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