The title compound, C(19)H(18)N(4)O(2), crystallizes with two independent mol-ecules in the asymmetric unit. The triazole ring is inclined to the benzene rings by 9.63â (13) and 87.37â (12)° in one mol-ecule, and by 4.46â (13) and 86.15â (11)° in the other. In the crystal, classical N-Hâ¯N hydrogen bonds, weak C-Hâ¯O hydrogen bonds and weak C-Hâ¯Ï inter-actions link the mol-ecules into a three-dimensional supra-molecular network. Hirshfeld surface analysis and two-dimensional fingerprint plots were used to investigate the inter-molecular inter-actions present in the crystal, indicating that the most important contributions for the crystal packing are from Hâ¯H (51.4%), Hâ¯C/Câ¯H (26.7%), Hâ¯O/Oâ¯H (8.9%) and Hâ¯N/Nâ¯H (8%) inter-actions.
Hirshfeld surface analysis and crystal structure of 7-meth-oxy-5-methyl-2-phenyl-11,12-di-hydro-5,11-methano-1,2,4-triazolo[1,5-c][1,3,5]benzoxadiazo-cine.
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作者:Gumus Mustafa Kemal, Kansiz Sevgi, Dege Necmi, Kalibabchuk Valentina A
| 期刊: | Acta Crystallographica Section E: Crystallographic Communications | 影响因子: | 0.500 |
| 时间: | 2018 | 起止号: | 2018 Aug 10; 74(Pt 9):1211-1214 |
| doi: | 10.1107/S2056989018010848 | ||
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