In the title compound, C(24)H(18)Cl(3)NO(3), the tetra-hydro-furan rings adopt envelope conformations. In the crystal, C-Hâ¯O hydrogen bonds connect mol-ecules, generating layers parallel to the (001) plane. These layers are connected along the c-axis direction by C-Hâ¯Ï inter-actions. The packing is further stabilized by inter-layer van der Waals and inter-halogen inter-actions. The most important contributions to the surface contacts are from Hâ¯H (36.8%), Clâ¯H/Hâ¯Cl (26.6%), Câ¯H/Hâ¯C (18.8%) and Oâ¯H/Hâ¯O (11.3%) inter-actions, as concluded from a Hirshfeld surface analysis.
Crystal structure and Hirshfeld surface analysis of 2,2,2-tri-chloro-N,N-bis-{[(1RS,4SR)-1,4-di-hydro-1,4-ep-oxy-naphthalen-1-yl]meth-yl}acetamide.
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作者:AtioÄlu Zeliha, Akkurt Mehmet, Mammadova Gunay Z, Bhattarai Ajaya
| 期刊: | Acta Crystallographica Section E: Crystallographic Communications | 影响因子: | 0.500 |
| 时间: | 2021 | 起止号: | 2021 Sep 28; 77(Pt 10):1048-1053 |
| doi: | 10.1107/S2056989021009907 | ||
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