â¢The aim of this work was to develop the methods of determination for phenol derivatives: bisphenol A (BPA), 4-tert-octylphenol (OP) and 4-nonylphenol (NP), in the whole body of herring Clupea harengus and in physiological fluids of the Baltic grey seal Halichoerus grypus grypus (blood and milk).â¢Methods were based on liquid chromatography coupled with a fluorescence detector (HPLC-FL).â¢These methods were satisfactorily validated, each showing good recovery (>80%) and precision (RSDâ<â15%). Regarding the limit of quantification (LOQ), this was established at <2 ngâg(-1) for herring, <0.07 ngâcm(-3) for blood and <0.1 ngâcm(-3) for milk.
Analytical methods for determination of bisphenol A, 4-tert-octylphenol and 4-nonylphenol in herrings and physiological fluids of the grey seal.
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作者:Staniszewska Marta, Nehring Iga, Falkowska Lucyna, Bodziach Karina
| 期刊: | MethodsX | 影响因子: | 1.900 |
| 时间: | 2018 | 起止号: | 2018 Sep 21; 5:1124-1128 |
| doi: | 10.1016/j.mex.2018.09.007 | ||
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