The redetermined structure of title chalcone derivative, C(23)H(16)O(2), corrects errors in the title, scheme and synthesis in the previous report of the same structure [Jasinski et al. (2011 â¶). Acta Cryst. E67, o795]. There are two independent mol-ecules in the asymmetric unit with slight differences in bond lengths and angles. The dihedral angle between the benzene ring and the anthracene ring system is 73.30â (4)° in one mol-ecule and 73.18â (4)° in the other. Both mol-ecules feature an intra-molecular O-Hâ¯O hydrogen bond, which generates an S(6) ring. In the crystal, mol-ecules are arranged into sheets lying parallel to the ac plane and further stacked along the b axis by Ï-Ï inter-actions with centroid-centroid distances in the range 3.6421â (6)-3.7607â (6)â à . The crystal structure is further stabilized by C-Hâ¯Ï inter-actions. There are also Câ¯O [3.2159â (15)â à ] short contacts.
Redetermination of (E)-3-(anthracen-9-yl)-1-(2-hy-droxy-phen-yl)prop-2-en-1-one.
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作者:Chantrapromma Suchada, Kobkeatthawin Thawanrat, Chanawanno Kullapa, Joothamongkhon Jaruwan, Fun Hoong-Kun
| 期刊: | Acta Crystallographica Section E-Structure Reports Online | 影响因子: | 0.600 |
| 时间: | 2011 | 起止号: | 2011 Oct 1; 67(Pt 10):o2554-5 |
| doi: | 10.1107/S1600536811034994 | ||
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