The asymmetric unit of the title compound, C17H17N3O2S, consists of two independent mol-ecules, A and B, with different conformations: in mol-ecule A, the dihedral angles between the central benzene ring and the pendant tolyl and carbamo-thio-ylhydrazono groups are 71.12â (9) and 5.95â (8)°, respectively. The corresponding angles in mol-ecule B are 50.56â (12) and 26.43â (11)°, respectively. Both mol-ecules feature an intra-molecular N-Hâ¯N hydrogen bond, which closes an S(5) ring. In the crystal, mol-ecules are linked by N-Hâ¯O, N-Hâ¯S and C-Hâ¯O hydrogen bonds, generating a three-dimensional network.
Crystal structure of (E)-4-{1-[2-(car-bamo-thio-yl)hydrazin-1-yl-idene]ethyl}phenyl 4-methyl-benzoate.
阅读:7
作者:Mani Karthik Ananth, Viswanathan Vijayan, Narasimhan S, Velmurugan Devadasan
| 期刊: | Acta Crystallographica Section E: Crystallographic Communications | 影响因子: | 0.500 |
| 时间: | 2015 | 起止号: | 2015 Jan 1; 71(Pt 1):o43-4 |
| doi: | 10.1107/S2056989014026942 | ||
特别声明
1、本页面内容包含部分的内容是基于公开信息的合理引用;引用内容仅为补充信息,不代表本站立场。
2、若认为本页面引用内容涉及侵权,请及时与本站联系,我们将第一时间处理。
3、其他媒体/个人如需使用本页面原创内容,需注明“来源:[生知库]”并获得授权;使用引用内容的,需自行联系原作者获得许可。
4、投稿及合作请联系:info@biocloudy.com。
