The title compound, C(25)H(29)NO(4)S(2) 0.5CH(2)Cl(2), was obtained as a racemate. The pyridine and phenyl rings are arranged face-to-face, giving a weak intra-molecular Ï-Ï inter-action [centroid-centroid separation = 3.759â (3)â Ã ]. These inter-actions are extended inter-molecularly, forming chains of stacked rings along [001] with separations of 3.859â (3) and 3.916â (3)â Ã . The solvent used for crystallization, CH(2)Cl(2), is located in voids between the chains of mol-ecules, with a site occupancy of 0.5.
(2SR,3RS)-Methyl 2-(adamantan-1-yl)-3-phenyl-sulfonyl-3-(pyridin-2-ylsulfan-yl)propano-ate dichloro-methane hemisolvate.
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作者:Meza-León Rosa-Luisa, Bernès Sylvain, RamÃrez DomÃnguez Elsie, Sosa-Rivadeneyra Martha, Quintero-Cortés Leticia
| 期刊: | Acta Crystallographica Section E-Structure Reports Online | 影响因子: | 0.600 |
| 时间: | 2011 | 起止号: | 2011 Apr 1; 67(Pt 4):o981-2 |
| doi: | 10.1107/S1600536811010312 | ||
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