The asymmetric unit of the title compound, C22H18N4O2S2, contains two mol-ecules. In one of them, the dihedral angles between the central benzene ring and the phenyl rings are 16.97â (8) and 20.97â (8)°, while the phenyl rings make a dihedral angle of 37.87â (8)°. In the other mol-ecule, the corresponding values are 34.92â (7), 53.90â (7) and 60.68â (8)°, respectively. In each mol-ecule, two intra-molecular N-Hâ¯O hydrogen bonds generate S(6) rings and a short C-Hâ¯S contact also occurs. In the crystal, N-Hâ¯S, N-Hâ¯O, C-Hâ¯O and C-Hâ¯S inter-actions link the mol-ecules into a three-dimensional network.
N,N'-Bis(phenyl-carbamo-thio-yl)benzene-1,3-dicarboxamide.
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作者:Ngaini Zainab, Mohd Ariff Maya Asyikin, Wan Zullkiplee Wan Sharifatun Handayani, Hussain Hasnain, Rosli Mohd Mustaqim
| 期刊: | Acta Crystallographica Section E-Structure Reports Online | 影响因子: | 0.600 |
| 时间: | 2013 | 起止号: | 2013 Aug 3; 69(Pt 9):o1374-5 |
| doi: | 10.1107/S1600536813020163 | ||
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