N-(4-Chloro-phen-yl)-4-meth-oxy-3-(propanamido)-benzamide cyclo-hexane hemisolvate.

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作者:Zhong Zhaojin, Li Zhuorong, Gong Ningbo, Li Yanping
The title compound, C(17)H(17)ClN(2)O(3)·0.5C(6)H(12), was prepared by the condensation reaction of 4-meth-oxy-3-(propanamido)-benzoic acid with 4-chloro-aniline. The Cl atom, the propionyl CH(3) group and the cyclo-hexyl CH(2) group are disordered over two sets of sites of equal occupancy in both mol-ecules. The cyclo-hexane solvent mol-ecule is disordered over two orientations which were modelled with relative occupancies of 0.484†(4) and 0.516†(4). In the crystal, there are a number of N-H⋯O hydrogen bonds, forming layers perpendicular to (001).

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