In the mol-ecule of the title compound, C(14)H(20)N(4)O(3), the five-membered ring adopts an envelope conformation with the O atom displaced by 0.207â (3)â à from the plane of the other ring atoms. Intra-molecular C-Hâ¯O hydrogen bonds result in the formation of three five-membered rings having envelope conformations. In the crystal structure, inter-molecular N-Hâ¯O hydrogen bonds link the mol-ecules, forming R(2) (2)(20) ring motifs, which produce two-dimensional polymeric sheets extending along the b axis. There are also two C-Hâ¯Ï inter-actions. The H atoms of one of the methyl groups are disordered over two positions and were refined with occupancies of 0.50.
(1R,3S)-1,1'-(1,3-Dihydro-2-benzofuran-1,3-diyl)bis(1,3-dimethyl-urea).
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作者:Maliha Bushra, Tariq Muhammad Ilyas, Tahir M Nawaz, Hussain Ishtiaq, Siddiqui Hamid Latif
| 期刊: | Acta Crystallographica Section E-Structure Reports Online | 影响因子: | 0.600 |
| 时间: | 2008 | 起止号: | 2008 Dec 6; 65(Pt 1):o42-3 |
| doi: | 10.1107/S1600536808040828 | ||
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