In the main mol-ecule of the title compound, C(22)H(20)N(2)O(4)·1.13CH(4)O, the dihedral angles between the benzimidazole plane and the two benzene rings are 80.53â (10) and 82.76â (10)°. The solvent mol-ecules are disordered between three positions, with refined occupancies of 0.506â (13), 0.373â (13) and 0.249â (5). The crystal structure is stabilized by inter-molecular O-Hâ¯O, O-Hâ¯N and C-Hâ¯O hydrogen bonds. The crystal studied was a merohedral twin [BASF ratio of 0.917â (1)/0.083â (1)].
2-[1-(2-Hydr-oxy-3-methoxy-benz-yl)-1H-benzimidazol-2-yl]-6-methoxy-phenol methanol 1.13-solvate.
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作者:Al-Douh Mohammed H, Osman Hasnah, Hamid Shafida A, Kia Reza, Fun Hoong-Kun
| 期刊: | Acta Crystallographica Section E-Structure Reports Online | 影响因子: | 0.600 |
| 时间: | 2009 | 起止号: | 2009 Mar 31; 65(Pt 4):o925-6 |
| doi: | 10.1107/S1600536809011192 | ||
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