In the title compound, C(14)H(11)N(3)OS·C(2)H(5)OH, the dihedral angle between the pyridine N-C(fused)-C(fused)-C(thio-phene) plane and the plane of the thio-phene ring is 81.9â (3)°, indicating that they are close to perpendicular. The dihedral angle between this pyridine plane and the benzene ring is 1.3â (3)°. The thio-phene ring is disordered over two coplanar orientations with an occupancy ratio of 0.692â (7):0.308â (7), while the ethanol solvent mol-ecule is also disordered over two sets of site in a 0.66â (4):0.34â (4) ratio. In the crystal, chains are formed along the b axis by N-Hâ¯O and O-Hâ¯N inter-actions with adjacent chains being connected through C-Hâ¯N and C-Hâ¯S inter-actions.
9-(Thio-phen-2-yl)-8,9-dihydro-3H-pyrazolo-[4,3-f]quinolin-7(6H)-one ethanol monosolvate.
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作者:Peng Juhua, Jia Runhong
| 期刊: | Acta Crystallographica Section E-Structure Reports Online | 影响因子: | 0.600 |
| 时间: | 2012 | 起止号: | 2012 Sep 1; 68(Pt 9):o2608 |
| doi: | 10.1107/S1600536812033533 | ||
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