The title compound, C(12)H(13)NO(4), was prepared as a precursor to an indole derivative with possible anti-mitotic properties. The mol-ecule is very nearly planar; the maximum deviation of any non-H atom from the mean plane of the indole ring is 0.120â (3)â à for each of two meth-oxy C atoms. The pairs of mol-ecules related by the inversion centre at (0,0,) are connected by two symmetry-equivalent N-Hâ¯O hydrogen bonds, while the pairs of mol-ecules related by the inversion centre at (0,0,0) exhibit a Ï-stacking inter-action of the indole rings, with an inter-planar separation of 3.39â (3)â à .
Methyl 5,6-dimeth-oxy-1H-indole-2-carboxyl-ate.
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作者:Monroe Thomas Blake, Moazami Yasamin, Jones Daniel S, Ogle Craig A
| 期刊: | Acta Crystallographica Section E-Structure Reports Online | 影响因子: | 0.600 |
| 时间: | 2009 | 起止号: | 2009 Sep 5; 65(Pt 10):o2353 |
| doi: | 10.1107/S1600536809034667 | ||
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