Crystals of the title compound, C(12)H(10)N(4)O(5), were obtained from a condensation reaction of 2,4-dinitro-phenyl-hydrazine and 2-furyl methyl ketone. The mol-ecule displays a nearly planar structure, and the furan ring is slightly twisted by a dihedral angle of 12.62â (6)° with respect to the phenyl-hydrazone plane. The face-to-face separation of 3.287â (7)â à between parallel benzene rings of adjacent mol-ecules indicates the existence of Ï-Ï stacking between dinitro-phenyl rings in the crystal structure.
(E)-2-Furyl methyl ketone 2,4-dinitro-phenyl-hydrazone.
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作者:Shan Shang, Tian Yu-Liang, Wang Shan-Heng, Wang Wen-Long, Xu Ying-Li
| 期刊: | Acta Crystallographica Section E-Structure Reports Online | 影响因子: | 0.600 |
| 时间: | 2008 | 起止号: | 2008 May 24; 64(Pt 6):o1153 |
| doi: | 10.1107/S1600536808015122 | ||
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