In the title compound, C(16)H(14)N(2)O(3)·4H(2)O, the dihedral angle between the mean planes of the benzimidazole ring system and benzene ring is 2.9â (1)°. The aldehyde group is disordered over two sets of sites with refined occupancies of 0.559â (4) and 0.441â (4). In the crystal, extensive inter-molecular O-Hâ¯O, O-Hâ¯N and N-Hâ¯O hydrogen bonds in concert with weak Ï-Ï stacking inter-actions [centroid-centroid distances = 3.6104â (9), 3.6288â (9) and 3.9167â (10)â à ] create a three-dimensional network.
4-(1H-Benzimidazol-2-ylmeth-oxy)-3-meth-oxy-benzaldehyde tetra-hydrate.
阅读:15
作者:Jasinski Jerry P, Golen James A, Samshuddin S, Narayana B, Yathirajan H S
| 期刊: | Acta Crystallographica Section E-Structure Reports Online | 影响因子: | 0.600 |
| 时间: | 2011 | 起止号: | 2011 Aug 1; 67(Pt 8):o2021-2 |
| doi: | 10.1107/S1600536811027164 | ||
特别声明
1、本页面内容包含部分的内容是基于公开信息的合理引用;引用内容仅为补充信息,不代表本站立场。
2、若认为本页面引用内容涉及侵权,请及时与本站联系,我们将第一时间处理。
3、其他媒体/个人如需使用本页面原创内容,需注明“来源:[生知库]”并获得授权;使用引用内容的,需自行联系原作者获得许可。
4、投稿及合作请联系:info@biocloudy.com。
