In the title compound, C22H19ClN2O3S, the dihedral angle between the mean planes of the thio-phene ring and the chloro-phenyl and hy-droxy-phenyl rings are 70.1â (1) and 40.2â (4)°, respectively. The benzene rings are twisted with respect to each other by 88.9â (3)°. The imine bond lies in an E conformation. Intra-molecular O-Hâ¯N and N-Hâ¯O hydrogen bonds each generate S(6) ring motifs. In the crystal, weak C-Hâ¯O inter-actions link the mol-ecules, forming chains along the c axis and zigzag chains along the b axis, generating sheets lying parallel to (100).
Crystal structure of N-[3-(2-chloro-benzo-yl)-5-ethyl-thio-phen-2-yl]-2-[(E)-(2-hy-droxy-benzyl-idene)amino]-acetamide.
N-[3-(2-氯苯甲酰基)-5-乙基噻吩-2-基]-2-[(E)-(2-羟基苄基亚甲基)氨基]-乙酰胺的晶体结构
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作者:Kaur Manpreet, Jasinski Jerry P, Kavitha Channappa N, Yathirajan Hemmige S, Byrappa K
| 期刊: | Acta Crystallographica Section E-Structure Reports Online | 影响因子: | 0.600 |
| 时间: | 2014 | 起止号: | 2014 Aug 16; 70(Pt 9):o1011-2 |
| doi: | 10.1107/S1600536814018224 | ||
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