In the title hydrazonodithio-ate, C(21)H(19)N(3)OS(2), the amide group is twisted out of the plane through the S(2)C=N atoms: the C-N-N-C torsion angle is 139.71â (13)°. The pyridine ring forms dihedral angles of 52.96â (8) and 86.46â (8)° with the phenyl rings, and the latter are approximately orthogonal [dihedral angle = 76.42â (9)°]. Supra-molecular chains sustained by N-Hâ¯O hydrogen bonds and propagated by glide symmetry along the c axis are found in the crystal structure. The chains are consolidated into a three-dimensional architecture by C-Hâ¯O and C-Hâ¯N inter-actions.
N'-[Bis(benzyl-sulfan-yl)methyl-idene]benzohydrazide.
N'-[双(苄基硫基)亚甲基]苯甲酰肼
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作者:Tayamon Shahedeh, Ravoof Thahira Begum S A, Tahir Mohamed Ibrahim Mohamed, Crouse Karen A, Tiekink Edward R T
| 期刊: | Acta Crystallographica Section E-Structure Reports Online | 影响因子: | 0.600 |
| 时间: | 2012 | 起止号: | 2012 Jun 1; 68(Pt 6):o1640-1 |
| doi: | 10.1107/S1600536812019472 | ||
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