In the title compound, C(16)H(14)N(2)O(4), the dihedral angle between the aromatic rings is 12.45â (6)°. The central C(=O)-N-N=C bridge is roughly planar (r.m.s. deviation = 0.0346â à ) and makes dihedral angles of 13.01â (7) and 0.56â (7)° with the attached phenyl and benzene rings, respectively. The acetic acid unit (r.m.s. deviation = 0.0066â à ) is twisted from its attached benzene ring [dihedral angle = 19.48â (6)°]. In the crystal, mol-ecules are linked by O-Hâ¯(O,N), N-Hâ¯O and C-Hâ¯O hydrogen bonds into sheets lying parallel to the bc plane. A weak aromatic Ï-Ï stacking inter-action is also observed [centroid-centroid distance = 3.7330â (7)â à ].
2-{2-[(E)-(2-Benzoyl-hydrazin-1-yl-idene)meth-yl]phen-oxy}acetic acid.
2-{2-[(E)-(2-苯甲酰肼-1-亚基)甲基]苯氧基}乙酸
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作者:Fun Hoong-Kun, Chia Tze Shyang, Alafeefy Ahmed M, Abdel-Aziz Hatem A
| 期刊: | Acta Crystallographica Section E-Structure Reports Online | 影响因子: | 0.600 |
| 时间: | 2012 | 起止号: | 2012 Jul 1; 68(Pt 7):o2260-1 |
| doi: | 10.1107/S1600536812028735 | ||
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