The title compound, C(24)H(19)NO, was obtained via the reaction of (1E,2E)-3-(3-meth-oxy-phen-yl)-1-phenyl-prop-2-en-1-one with ethyl 2-oxo-propano-ate, using NH(4)I as a catalyst. The compound crystallizes in the monoclinic space group I2/a. In the mol-ecule, the four rings are not in the same plane, the pyridine ring being inclined to the benzene rings by 17.26â (6), 56.16â (3) and 24.50â (6)°. In the crystal, mol-ecules are linked by C-Hâ¯Ï inter-actions into a three-dimensional network. To further analyse the inter-molecular inter-actions, a Hirshfeld surface analysis was performed. Hirshfeld surface analysis indicates that the most abundant contributions to the crystal packing are from Hâ¯H (50.4%), Câ¯H/Hâ¯C (37.9%) and Oâ¯H/Hâ¯O (5.1%) inter-actions.
Crystal structure and Hirshfeld surface analysis of 4-(3-meth-oxy-phen-yl)-2,6-di-phenyl-pyridine.
阅读:3
作者:Cheng Dong, Meng Xiang-Zhen, Tian Fuyu, Yan Dong, Wang Xiaofei, Qian Xueli, Wang Junnan
| 期刊: | Acta Crystallographica Section E: Crystallographic Communications | 影响因子: | 0.500 |
| 时间: | 2022 | 起止号: | 2022 Aug 23; 78(Pt 9):932-935 |
| doi: | 10.1107/S2056989022007812 | ||
特别声明
1、本文转载旨在传播信息,不代表本网站观点,亦不对其内容的真实性承担责任。
2、其他媒体、网站或个人若从本网站转载使用,必须保留本网站注明的“来源”,并自行承担包括版权在内的相关法律责任。
3、如作者不希望本文被转载,或需洽谈转载稿费等事宜,请及时与本网站联系。
4、此外,如需投稿,也可通过邮箱info@biocloudy.com与我们取得联系。
