In the title compound, C(30)H(31)NO(3)S(2), the piperidine ring adopts a distorted chair conformation. The thio-phene rings have twisted conformations about the C-C bonds. The mean plane of the piperidine ring makes a near orthogonal conformation with the toluene ring. Two of the phenyl rings in the structure are positionally disordered over two sets of sites with occupancies of 0.56â (2)/0.44â (2) and 0.672â (16)/0.328â (16). A region of disordered electron density was corrected for using the SQUEEZE [Spek (2015 â¸). Acta Cryst. C71, 9-18] routine in PLATON. The given chemical formula and other crystal data do not take into account the unknown solvent mol-ecule. In the crystal, O-Hâ¯O hydrogen bonds are observed along with intra-molecular Sâ¯H, Oâ¯H, Câ¯H and Hâ¯H contacts.
13-Benzyl-4,11-dihy-droxy-1,8-diphen-yl-2,9-di-thia-13-aza-dispiro-[4.1.4.3]tetra-decan-6-one.
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作者:Vinotha G, Sundar T V, Sharmila N
| 期刊: | IUCrdata | 影响因子: | 0.000 |
| 时间: | 2021 | 起止号: | 2021 Feb 26; 6(Pt 2):x210210 |
| doi: | 10.1107/S2414314621002108 | ||
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