Novel (iPr)Ru-MACHO Salts: Synthesis and Catalytic Applications With Diverse H-Trans Ligands

新型(iPr)Ru-MACHO盐:合成及与多种H-反式配体的催化应用

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Abstract

The Ru-MACHO complex acts as a precatalyst for a plethora of significant catalytic transformations. However, since its discovery approximately two decades ago, most enhancement attempts have been limited to varying the P-substituents for increasing catalyst performance or replacing Ru for greener alternatives. In this study we synthesize novel trans-L monohydrido (iPr)Ru-MACHO complex derivatives that can act as precatalysts operating under mild conditions while maintaining high activity and selectivity in a variety of chemical transformations. Specifically, we deeply studied their potentially trans influence and investigated their catalytic efficiency for CO(2) hydrogenation, formic acid dehydrogenation, and levulinic acid hydrogenation, and we compared their activity with their commercially available precursor ((iPr)Ru-MACHO).

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