In the footsteps of August Michaelis: Syntheses and Thermodynamics of Extremely Low-Volatile Ionic Liquids

追随奥古斯特·米凯利斯的脚步:超低挥发性离子液体的合成与热力学

阅读:1

Abstract

A series of nine different known ionic liquids or low melting salts was synthesised and purified. They are composed of the [NTf(2) ](-) (bis(trifluoromethane)sulfonimide), [OTf](-) (trifluoro-methane-sulfonate), or [B(CN)(4) ](-) (tetracyanidoborate) anion and [Ph(4) P](+) (tetraphenylphosphonium), [Ph(3) BzP](+) (triphenylbenzyl phosphonium), [(n) Bu(4) P](+) (tetra-(n) butylphosphonium), [(n) BuPh(3) P](+) (tri-phenyl-(n) butylphosphonium), [(n) Bu(4) N](+) (tetra-(n) butylammonium), or the [PPN](+) (bis(triphenylphosphine)iminium) cation. Precise vapour pressure data and enthalpies of vaporisation were measured using the Quartz Crystal Microbalance (QCM) method and evaluated. Structure-property relations are established using the obtained data as well as literature known data of ILs with alkyl-substituted imidazolium cations. It turns out that ILs with the tetracyanidoborate anion have even higher values of the enthalpy of vaporisation than those with the common [NTf(2) ](-) or [OTf](-) anion and therefore are even less volatile.

特别声明

1、本页面内容包含部分的内容是基于公开信息的合理引用;引用内容仅为补充信息,不代表本站立场。

2、若认为本页面引用内容涉及侵权,请及时与本站联系,我们将第一时间处理。

3、其他媒体/个人如需使用本页面原创内容,需注明“来源:[生知库]”并获得授权;使用引用内容的,需自行联系原作者获得许可。

4、投稿及合作请联系:info@biocloudy.com。