Electro-Co-Polymerisation of Polypyrrole-Polyaniline Composites in Ionic Liquids for Metal-Free Hydrogen Evolution Electrodes

离子液体中聚吡咯-聚苯胺复合材料的电共聚合及其在无金属析氢电极中的应用

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Abstract

Pure organic films consisting of polypyrrole, polyaniline and a composite of polypyrrole and polyaniline electrodeposited in the ionic liquid EMIM-TFSI onto mesoporous carbon electrodes are tested for their hydrogen evolution reaction capabilities. The use of these intrinsically conducting polymers is seen as a way of stepping away from expensive and rare metallic catalysts. Co-polymerisation of polypyrrole and polyaniline in a 1 : 10 ratio in EMIM-TFSI was found to be doped with the TFSI(-) anion and be much more active to the hydrogen evolution reaction when compared to pure polymers. Tafel analysis of the composite gave a value of 144 mV/dec indicating that the Volmer step is the rate limiting step. However, stability tests showed an improvement in the composite's overpoential performance for the hydrogen evolution reaction.

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