Ring-Opening Polymerization of rac-Lactide with Aluminum Chiral Anilido-Oxazolinate Complexes

利用手性铝苯胺基噁唑啉络合物催化外消旋丙交酯的开环聚合

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Abstract

A series of dimethylaluminum complexes (L(1a-i) )AlMe(2) (2a-i, where HL(1a-i) = 2-(2'-ArNH)phenyl-4-R(1)-oxazoline) bearing chiral, bidentate anilido-oxazolinate ligands have been prepared and characterized. Six of the complexes, in the presence of an alcohol cocatalyst, are shown to be active initiators for the stereoselective ring-opening polymerization of rac-lactide in toluene solution and under bulk conditions, yielding polylactides with a range of tacticity from slightly isotactic to moderately heterotactic. The reactivity and selectivity of these catalysts are discussed on the basis of the effect of their substituents.

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