(2,2'-Bipyrid-yl)(η(6)-p-cymene)iodidoruthenium(II) hexa-fluorido-phosphate

(2,2'-联吡啶基)(η(6)-对异丙基甲苯)碘化钌(II)六氟磷酸盐

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Abstract

The title compound, having the mol-ecular formula [RuI(η(6)-C(10)H(14))(C(10)H(8)N(2))]PF(6), crystallizes in the triclinic P (Z = 2) space group as a half-sandwich complex resembling a three-legged piano stool. Important geometrical parameters include Ru-cymene centroid = 1.6902 (17) Å, Ru-I = 2.6958 (5) Å, [Ru-N](avg) = 2.072 (3) Å, N1-Ru-N2 = 76.86 (12)° and a dihedral angle between the planes of the two rings of the bipyridyl system of 5.9 (2)°. The PF(6) (-) ion was treated with a twofold disorder model, refining to a 65.0 (8):35.0 (8) occupancy ratio. The crystal packing features C-H⋯F/I inter-actions.

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