Effects of post-polymerization conditions on color properties, surface roughness, and flexural strength of 3D-printed permanent resin material after thermal aging

热老化后聚合条件对3D打印永久树脂材料的颜色特性、表面粗糙度和弯曲强度的影响

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Abstract

PURPOSE: To evaluate the color, surface properties, and flexural strength of 3D-printed permanent crown resin subjected to different post-polymerization conditions after artificial aging. MATERIALS AND METHODS: Ninety (10 × 2 mm) disc-shaped specimens were printed by using permanent crown resin with SLA technology. Specimens were divided into nine different groups, subject to post-polymerization conditions at three different times (15, 20, and 30 min) and three different temperatures (40, 60, and 80°C) (n = 10). Color and surface roughness measurements were repeated pre-post thermal aging (5.000 cycles, 5-55°C) and a flexural strength test was carried out. Data were analyzed with Shapiro-Wilk, Kruskal-Wallis, ANOVA, Tukey HSD, and Dunn tests (α < 0.05). RESULTS: ΔE(00) values showed results below the acceptable color threshold, except for the 30 min 40°C group (ΔE(00) <1.8). No difference was found between the relative translucency parameter and surface roughness values of the 20 min 60°C group recommended by the manufacturer and the other groups. A significant difference was found between the flexural strength values of the groups (p < 0.001). CONCLUSIONS: The color properties, surface topography, and mechanical properties of the printed permanent crown material were affected by different post-polymerization conditions: polymerized at different times and temperatures. Although the flexural strength and color change values showed promising results, more studies are required to evaluate its suitability for clinical use.

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