Atomic perspective elucidates mixed alcohol synthesis from syngas on bilayered (K)/MoS(2) catalysts

从原子角度阐明了在双层(K)/MoS(2)催化剂上由合成气合成混合醇的反应机理

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Abstract

Syngas serves as a crucial link between non-petroleum-based carbon resources and commodity chemicals. Among various conversion routes, the catalytic transformation of syngas into ethanol and other mixed alcohols represents a highly attractive option. K-modified MoS(2) systems exhibit notable activity and selectivity in low-carbon alcohol synthesis. To elucidate the correlation between product selectivity and catalyst structure, and to design efficient catalysts for the synthesis of specific single products, density functional theory (DFT) was employed to explore the transition states of elementary steps involved in syngas conversion to mixed alcohols on bilayer (K)/MoS(2) catalysts. The results indicate that CO hydrogenation on the S-edge sites of the MoS(2)(100) facet mainly yields C(1) species, whereas ethanol is primarily produced at the Mo-edge sites. Moreover, K doping enhances CO activation and C-C coupling at the Mo-edge. The most favorable pathway for ethanol synthesis at the Mo-edge is identified as CO → HCO → CHOH → CH → CHCO → CH(2)CO → CH(3)CO → CH(3)CHO → CH(3)CH(2)O → CH(3)CH(2)OH, with the key step being the hydrogenation of CH(3)CO to CH(3)CHO, which requires an energy barrier of 0.73 eV. This work offers comprehensive and valuable guidance for the subsequent modification and design of C-C coupling catalysts.

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