Crystal structure of a 1,1-dibutyl-1H,3H-naphtho[1,8-cd][1,2,6]oxastannaborinin-3-ol

1,1-二丁基-1H,3H-萘并[1,8-cd][1,2,6]氧杂锡硼烷-3-醇的晶体结构

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Abstract

The title oxastannaborininol compound, [Sn(C(4)H(9))(2)(C(10)H(7)BO(2))], has been synthesized and crystallized. While heterocycles containing a C-O-B group are common, heterocycles containing an E-O-B unit, where E is an element of the carbon group except for carbon, are rare. In fact, while heterocycles containing Si-O-B units are occasionally reported (although without crystal structures), there are no reports for the corresponding germanium, tin or lead analogues. Herein, the first synthesis and crystal structure of a heterocycle containing an Sn-O-B unit is described. The asymmetric unit contains one mol-ecule showing a notable disorder of the tin atom and the butyl groups. They occupy two sets of positions with site-occupancy factors of 0.295 (6) and 0.705 (6).

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