Visualization and validation of twin nucleation and early-stage growth in magnesium

镁中孪生成核和早期生长的可视化和验证

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作者:Lin Jiang, Mingyu Gong, Jian Wang, Zhiliang Pan, Xin Wang, Dalong Zhang, Y Morris Wang, Jim Ciston, Andrew M Minor, Mingjie Xu, Xiaoqing Pan, Timothy J Rupert, Subhash Mahajan, Enrique J Lavernia, Irene J Beyerlein, Julie M Schoenung

Abstract

The abrupt occurrence of twinning when Mg is deformed leads to a highly anisotropic response, making it too unreliable for structural use and too unpredictable for observation. Here, we describe an in-situ transmission electron microscopy experiment on Mg crystals with strategically designed geometries for visualization of a long-proposed but unverified twinning mechanism. Combining with atomistic simulations and topological analysis, we conclude that twin nucleation occurs through a pure-shuffle mechanism that requires prismatic-basal transformations. Also, we verified a crystal geometry dependent twin growth mechanism, that is the early-stage growth associated with instability of plasticity flow, which can be dominated either by slower movement of prismatic-basal boundary steps, or by faster glide-shuffle along the twinning plane. The fundamental understanding of twinning provides a pathway to understand deformation from a scientific standpoint and the microstructure design principles to engineer metals with enhanced behavior from a technological standpoint.

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