Isotopic Transient Kinetic Analysis of Soot Oxidation on Mn(3)O(4), Mn(3)O(4)-CeO(2), and CeO(2) Catalysts in Tight Contact Conditions

在紧密接触条件下,Mn(3)O(4)、Mn(3)O(4)-CeO(2)和CeO(2)催化剂上烟尘氧化的同位素瞬态动力学分析

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Abstract

The reaction mechanism of soot oxidation on Mn (Mn(3)O(4)), Mn-Ce (Mn(3)O(4)-CeO(2)), and Ce (CeO(2)) catalysts in tight contact conditions was investigated using ITKA (isotopic transient kinetic analysis). The obtained results suggest that lattice-bulk oxygen from all studied catalysts takes part in the soot oxidation process but with varying relative contributions: for the Ce catalyst, this contribution is practically 100%, whereas with decreasing Ce content in Mn-Ce catalysts, the significance of lattice-bulk oxygen for soot oxidation diminishes. For the Mn catalyst, it is estimated to be below 50%. Moreover, strong interactions between Mn and Ce ions were observed, increasing oxygen mobility in the catalyst crystal lattice and affecting the activity of Mn-Ce catalysts.

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