High crystallinity and polar-phase content in electrospun P(VDF-TrFE) nanofibers with low molecular weight

低分子量电纺P(VDF-TrFE)纳米纤维具有高结晶度和极性相含量

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Abstract

Electrospun piezoelectric nanofibers from polyvinylidene fluoride (PVDF) have been widely used in many applications. In PVDF-based polymers, the molecular weight (M(w)) plays an important role in determining both crystallization and polarization responses. In the past, polyvinylidene fluoride trifluoroethylene [P(VDF-TrFE)] electrospun nanofibers were produced strictly from high molecular weight polymers (M(w) > 200 kDa). Here, we study the electrospun P(VDF-TrFE) nanofibers from comparatively lower M(w) polymers (M(w) ∼ 100 kDa). We demonstrated a highly electroactive phase in electrospun P(VDF-TrFE) nanofibers without post treatments. During electrospinning, shorter P(VDF-TrFE) polymer chains exhibited higher mobility, which facilitate the formation of all-trans ferroelectric crystals with high crystallinity. By optimizing the mean size of electrospun nanofiber through tailoring the solution concentration and other controlling parameters, P(VDF-TrFE) nanofibers achieved the crystallinity as high as 67% and all-trans conformation reached 79%. The results pave a way for improving the electroactive performance in ferroelectric polymer electrospun nanofibers.

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