Synthesis and Characterisation of Metal-Glass Composite Materials Fabricated by Liquid Phase Sintering

液相烧结法制备金属-玻璃复合材料的合成与表征

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Abstract

In recent years, there has been a global increase in environmental awareness, which has driven the application of natural materials or the synthesis of novel, environmentally compatible materials. Composite materials hold a prominent position among modern materials and are typically developed to achieve resistance to various damage mechanisms, thereby extending the service life of structures. This study presents the synthesis and characterisation of high-density metal-glass composite materials. The commercially available 316L stainless steel powder was used as the matrix material, while andesite basalt powder was used as the reinforcement phase. Andesite basalt aggregate, ground into powder, is a cost-effective, widely available, and environmentally friendly natural raw material. Powder metallurgy was employed to produce the composite materials. Sintering was performed at 1250 °C for 30 min in a vacuum. The density of the sintered composite samples was analysed as a function of andesite basalt content, with sintering conducted in the presence of a liquid phase. Composite materials were characterised using optical and scanning electron microscopy, X-ray structural analysis, and hardness testing. This study confirmed that the optimal combination of properties was achieved in the composite with 20 wt.% andesite basalt, present as a glass phase within the 316L steel matrix.

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