Synthesis and Structure-Activity Relationship Study of 2-(amino)quinazolin-4(3H)-one Derivatives as Potential Inhibitors of Methicillin-Resistant Staphylococcus aureus (MRSA)

2-(氨基)喹唑啉-4(3H)-酮衍生物作为耐甲氧西林金黄色葡萄球菌(MRSA)潜在抑制剂的合成及构效关系研究

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Abstract

Background/Objectives: The rise in methicillin-resistant Staphylococcus aureus (MRSA) demands new therapeutic strategies. In this study, a series of 2-(amino)quinazolin-4(3H)-one derivatives were synthesized and evaluated for antistaphylococcal activity. Methods/Results: Through screening against S. aureus ATCC25923 and USA300 JE2, several submicromolar inhibitors were identified. Among them, compound 6l, which contains a 7-chloro substituent on the key parental scaffold, exhibited strong overall antibacterial activity (MIC(50): 1.0 µM, ATCC25923; 0.6 µM, JE2) and served as a lead for further structural optimization. Structure-activity relationship analysis showed that substitution at the 2-position was critical, with its optimized analog 6y (3,4-difluorobenzylamine) exhibiting the highest potency (MIC(50): 0.36 µM, ATCC25923; 0.02 µM, JE2). Cytotoxicity assays in HepG2 cells revealed six compounds with IC(50) values above 20 µM, yielding efficacy windows greater than 10. Compound 6y exhibited an exceptional index (~885). Consistently, in an H460 lung epithelial infection model mimicking MRSA pneumonia, 6y significantly reduced intracellular bacterial loads with minimal host cell damage, outperforming comparator compounds. Conclusions: These findings highlight 2-(amino)quinazolin-4(3H)-one derivatives, particularly 6y, as promising leads for the development of new antistaphylococcal agents.

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