Investigation of Electronic Structures of Triplet States Using Step-Scan Time-Resolved Fourier-Transform Near-Infrared Spectroscopy

利用步进扫描时间分辨傅里叶变换近红外光谱研究三重态的电子结构

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Abstract

Triplet transitions of light-emitting materials, including rose bengal, tris(2-phenylpyridine)iridium(III) [Ir(ppy)(3)], tris(1-phenylisoquinoline)iridium(III) [Ir(piq)(3)], and bis[2-(4,6-difluorophenyl)pyridinato-C2,N](picolinato)iridium(III) (FIrpic), were studied using step-scan time-resolved Fourier-transform near-infrared spectroscopy. The samples were excited to their singlet excited states by a 355 nm laser and then underwent efficient conversions/crossings to their triplet manifolds. For rose bengal, a transient absorption band appeared at 9400 cm(-1), attributed to the T(3) ← T(1) transition based on the corresponding time evolution and the theoretical calculations. For Ir(ppy)(3), Ir(piq)(3), and FIrpic, the most intense bands were observed at 7700, 7500, and 7500 cm(-1) and assigned to T(7) ← T(1), T(6) ← T(1), and T(6) ← T(1) transitions, respectively. For Ir(ppy)(3), the most intense band involved transitions between different triplet metal-to-ligand charge transfer ((3)MLCT) states, while for Ir(piq)(3) and FIrpic, they involved a metal center to (3)MLCT transition. These T(1) states were assigned to (3)MLCT.

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