Deciphering the doublet luminescence mechanism in neutral organic radicals: spin-exchange coupling, reversed-quartet mechanism, excited-state dynamics

解析中性有机自由基的双线态发光机制:自旋交换耦合、反向四重态机制、激发态动力学

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Abstract

Neutral organic radical molecules have recently attracted considerable attention as promising luminescent and quantum-information materials. However, the presence of a radical often shortens their excited-state lifetime and results in fluorescence quenching due to enhanced intersystem crossing (EISC). Recently, an experimental report introduced an efficient luminescent radical molecule, tris(2,4,6-trichlorophenyl)methyl-carbazole-anthracene (TTM-1Cz-An). In this study, we systematically performed quantum theoretical calculations combined with the path integral approach to quantitatively calculate the excited-state dynamics processes and spectral characteristics. Our theoretical findings suggest that the sing-doublet D(1) state, originating from the anthracene excited singlet state, is quickly converted to the doublet (trip-doublet) state via EISC, facilitated by a significant nonequivalence exchange interaction, with ΔJ (ST) = 0.174 cm(-1). The formation of the quartet state (Q(1), trip-quartet) was predominantly dependent on the exchange coupling 3/2J (TR) = 0.086 cm(-1) between the triplet spin electrons of anthracene and the TTM-1Cz radical. Direct spin-orbit coupling ISC to the Q(1) state was minimal due to the nearly identical spatial wavefunctions of the and Q(1) levels. The effective occurrence of reverse intersystem crossing (RISC) from the Q(1) to D(1) state is a critical step in controlling the luminescence of TTM-1Cz-An. The calculated RISC rate k (RISC), including the Herzberg-Teller effect, was 3.64 × 10(5) s(-1) at 298 K, significantly exceeding the phosphorescence and nonradiative rates of the Q(1) state, thus enabling the D(1) repopulation. Subsequently, a strong electronic coupling of 37.4 meV was observed between the D(1) and D(2) states, along with a dense manifold of doublet states near the D(1) state energy, resulting in a larger reverse internal conversion rate k (RIC) of 9.26 × 10(10) s(-1). Distributed to the D(2) state, the obtained emission rate of k (f) = 2.98-3.18 × 10(7) s(-1) was in quite good agreement with the experimental value of 1.28 × 10(7) s(-1), and its temperature effect was not remarkable. Our study not only provides strong support for the experimental findings but also offers valuable insights for the molecular design of high-efficiency radical emitters.

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