Identifying competitive protein antagonists for F-actin with reverse-phase high-performance liquid chromatography

利用反相高效液相色谱法鉴定F-肌动蛋白的竞争性蛋白拮抗剂

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Abstract

F-actin binding constants are traditionally determined by centrifugal cosedimentation with actin microfilaments, where bound protein is separated from actin with SDS-PAGE and quantitated using densitometry. Here, we demonstrate that UV quantitation of reverse-phase HPLC-separated proteins provides increased accuracy and sensitivity, can be fully automated, and allows one to perform F-actin competition assays on similar sized proteins.

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