Integration of Non-Invasive Micro-Test Technology and (15)N Tracing Reveals the Impact of Nitrogen Forms at Different Concentrations on Respiratory and Primary Metabolism in Glycyrrhiza uralensis

非侵入性微型检测技术与 (15)N 示踪技术的结合揭示了不同浓度氮形态对甘草呼吸作用和初级代谢的影响

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Abstract

Glycyrrhiza uralensis is a highly valued medicinal species worldwide. However, a paradox arises in its cultivation in that high nitrogen fertilization boosts yield at the expense of root quality, a problem linked to nitrogen's regulation of tricarboxylic acid (TCA) cycle-driven respiration. It remains unclear how different nitrogen forms coordinate respiratory and primary metabolism. We examined the regulatory mechanisms of nitrate (NO(3)(-)) versus ammonium (NH(4)(+)) on these processes in cultivated G. uralensis by supplying seedlings with varying concentrations of K(15)NO(3) or ((15)NH(4))(2)SO(4) in a modified Hoagland solution (HNS). Using non-invasive micro-test technology (NMT) and (15)N tracing, we found that G. uralensis employs distinct nitrogen acquisition strategies: sustaining uptake at optimal NH(4)(+) and low-to-moderate NO(3)(-), while declining uptake under high NO(3)(-). These strategies drove form-specific differences in the activity of key nitrogen assimilation enzymes, nitrate reductase and nitrite reductase (NR/NiR), as well as glutamine synthetase and glutamate synthase (GS/GOGAT), and subsequent glutamate and glutamine accumulation. Ammonium nutrition enhanced primary ammonia assimilation and gamma-aminobutyric acid (GABA) metabolism, leading to greater glutamate and endogenous GABA levels. In contrast, nitrate nutrition preferentially stimulated the TCA cycle, resulting in higher accumulation of α-ketoglutarate (KGA) and succinate. The concomitant increase in GABA catabolism supported this nitrogen-responsive respiratory metabolism, acting as a compensatory mechanism to maintain KGA homeostasis. Our findings inform nitrogen form strategies for G. uralensis cultivation.

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