Crystal structure, Hirshfeld surface analysis, DFT and mol-ecular docking studies of ethyl 5-amino-2-bromo-isonicotinate

5-氨基-2-溴异烟酸乙酯的晶体结构、Hirshfeld表面分析、DFT计算和分子对接研究

阅读:3

Abstract

In the title compound, C(8)H(9)BrN(2)O(2), the C-O-C-C torsion angle between isonicotine and the ethyl group is 180.0 (2)°. Intra-molecular N-H⋯O and C-H⋯O inter-actions consolidate the mol-ecular structure. In the crystal, N-H⋯N inter-action form S(5) zigzag chains along [010]. The most significant contributions to the Hirshfeld surface arise from H⋯H (33.2%), Br⋯H/H⋯Br (20.9%), O⋯H/H⋯O (11.2%), C⋯H/H⋯C (11.1%) and N⋯H/H⋯N (10%) contacts. The topology of the three-dimensional energy frameworks was generated using the B3LYP/6-31 G(d,p) model to calculate the total inter-action energy. The net inter-action energies for the title compound are E (ele) = 59.2 kJ mol(-1), E (pol) = 15.5 kJ mol(-1), E (dis) = 140.3 kJ mol(-1) and E (rep) = 107.2 kJ mol(-1) with a total inter-action energy E (tot) of 128.8 kJ mol(-1). The mol-ecular structure was optimized by density functional theory (DFT) at the B3LYP/6-311+G(d,p) level and the theoretical and experimentally obtained parameters were compared. The frontier mol-ecular orbitals HOMO and LUMO were generated, giving an energy gap ΔE of 4.0931 eV. The MEP was generated to identify active sites in the mol-ecule and mol-ecular docking studies carried out with the title compound (ligand) and the covid-19 main protease PDB ID: 6LU7, revealing a moderate binding affinity of -5.4 kcal mol(-1).

特别声明

1、本页面内容包含部分的内容是基于公开信息的合理引用;引用内容仅为补充信息,不代表本站立场。

2、若认为本页面引用内容涉及侵权,请及时与本站联系,我们将第一时间处理。

3、其他媒体/个人如需使用本页面原创内容,需注明“来源:[生知库]”并获得授权;使用引用内容的,需自行联系原作者获得许可。

4、投稿及合作请联系:info@biocloudy.com。