Validation of three-dimensional diffraction contrast tomography reconstructions by means of electron backscatter diffraction characterization

通过电子背散射衍射表征验证三维衍射对比断层扫描重建

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作者:Melanie Syha, Andreas Trenkle, Barbara Lödermann, Andreas Graff, Wolfgang Ludwig, Daniel Weygand, Peter Gumbsch

Abstract

Microstructure reconstructions resulting from diffraction contrast tomography data of polycrystalline bulk strontium titanate were reinvestigated by means of electron backscatter diffraction (EBSD) characterization. Corresponding two-dimensional grain maps from the two characterization methods were aligned and compared, focusing on the spatial resolution at the internal interfaces. The compared grain boundary networks show a remarkably good agreement both morphologically and in crystallographic orientation. Deviations are critically assessed and discussed in the context of diffraction data reconstruction and EBSD data collection techniques.

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